DENSIFICATION AND MICROSTRUCTURE CHARACTERISTICS OF A PREALLOYED ALPHA BRASS POWDER PROCESSED BY LIQUID PHASE SINTERING

Authors

  • A. Mohammadzadeh Department of Materials Engineering, Sahand University of Technology, Tabriz, Iran.
  • A. Sabahi Namini Department of Materials Engineering, Sahand University of Technology, Tabriz, Iran.
  • M. Azadbeh Department of Materials Engineering, Sahand University of Technology, Tabriz, Iran.
Abstract:

The rapidly solidified prealloyed alpha brass powder with a size range of 40 to 100 μm produced by water atomization process was consolidated using liquid phase sintering process. The relationships between sintering temperature, physic-mechanical properties and microstructural characteristics were investigated. Maximum densification was obtained at 930 °C, under 600 MPa compacting pressure, with 60 min holding time. The microstructure of the sintered brass was influenced by dezincification and structural coarsening during supersolidus liquid phase sintering. As a consequence of Kirkendall effect atomic motion between Cu and Zn atoms caused to dezincification at the grain boundaries and formation of ZnO particles on the pore surfaces. It was concluded that microstructural analysis is in a well agreement with obtained physical and mechanical properties. Also, the amount of liquid phase, which depends on sintering temperature, results in different load bearing cross section areas, and it affects the type of fracture morphologies.

Upgrade to premium to download articles

Sign up to access the full text

Already have an account?login

similar resources

EFFECT OF SUPERSOLIDUS LIQUID PHASE SINTERING ON THE MICROSTRUCTURE AND DENSIFICATION OF THE Al-Cu-Mg PREALLOYED POWDER

Abstract: The supersolidus liquid phase sintering characteristics of commercial 2024 pre-alloyed powder was studied at different sintering conditions. Pre-alloyed 2024 aluminum alloy powder was produced via air atomizing process with particle size of less than 100 µm. The solidus and liquidus temperatures of the produced alloy were determined using differential thermal analysis (DTA). The sinte...

full text

Evaluation of Heterogeneous Densification, Anisotropic Shrinkage and Rheological Behavior of Ceramic Materials during Liquid Phase Sintering by Numerical-Experimental Procedure

The effective shear and bulk viscosity, as well as dynamic viscosity, describe the rheological properties of the ceramic body during the liquid phase sintering process. The rheological parameters depend on the physical and thermo-mechanical characteristics of the material such as relative density, temperature, grain size, diffusion coefficient, and activation energy. Thermal behavior of the cer...

full text

Microstructure and Mechanical Behavior of Porous Ti–6Al–4V Processed by Spherical Powder Sintering

Reducing the stiffness of titanium is an important issue to improve the behavior of this material when working together with bone, which can be achieved by generating a porous structure. The aim of this research was to analyze the porosity and mechanical behavior of Ti-6Al-4V porous samples developed by spherical powder sintering. Four different microsphere sizes were sintered at temperatures r...

full text

Finite element simulation of pyroplastic deformation, anisotropic shrinkage and heterogeneous densification for ceramic materials during liquid phase sintering process

Pyroplastic deformation is a distortion of the ceramic shape during the sintering process. It occurs because the flow of the vitreous phase at high temperature and the applied stress due to the weight of the product during sintering process. The aim of this paper deals with describing a numerical-experimental method to evaluate the pyroplastic deformation, to predict the anisotropic shrinkage a...

full text

An Update on the Theory of Supersolidus Liquid Phase Sintering

Prealloyed powders usually melt over a range of temperatures. This feature is useful in performing supersolidus liquid phase sintering, where liquid forms inside the particles when heated just over the solidus temperature. Densification by supersolidus liquid phase sintering is sensitive to time-temperatures. A major difficulty arises when a narrow temperature range exists between densification...

full text

Microstructure Evolution and Mechanical Properties Improvement in Liquid-Phase-Sintered Hydroxyapatite by Laser Sintering

CaO-Al₂O₃-SiO₂ (CAS) as a liquid phase was introduced into hydroxyapatite (HAp) to prepare bone scaffolds. The effects of the CAS content (1, 2, 3, 4 and 5 wt%) on microstructure and mechanical properties of HAp ceramics were investigated. The optimal compression strength, fracture toughness and Vickers hardness reached 22.22 MPa, 1.68 MPa·m1/2 and 4.47 GPa when 3 wt% CAS was added, which were ...

full text

My Resources

Save resource for easier access later

Save to my library Already added to my library

{@ msg_add @}


Journal title

volume 11  issue 3

pages  67- 74

publication date 2014-09

By following a journal you will be notified via email when a new issue of this journal is published.

Keywords

Hosted on Doprax cloud platform doprax.com

copyright © 2015-2023